An analytical chemistry laboratory session was conducted focusing on the Boiling Point determination experiment, under the supervision of Engineer Tabarak Mohsin Ashour, as part of enhancing the practical component of the academic curriculum and linking theoretical concepts with hands-on application. The experiment aimed to introduce students to the importance of boiling point as a fundamental physical property used in identifying pure substances and evaluating their purity, in addition to developing their skills in operating laboratory instruments, accurately recording measurements, and scientifically analyzing results, while emphasizing adherence to laboratory safety procedures. This scientific activity aligns with the Sustainable Development Goals (SDGs), particularly: SDG 4: Quality Education, by providing high-quality practical learning experiences. SDG 9: Industry, Innovation, and Infrastructure, through preparing qualified graduates to support scientific research and technological advancement. SDG 12: Responsible Consumption and Production, by promoting the safe and efficient use of chemical materials and reducing laboratory waste.