As part of the practical program of the Analytical Chemistry Laboratory, the Recrystallization experiment was conducted as one of the essential techniques used for purifying solid compounds and removing impurities, due to its significance in analytical and research applications. The experiment was carried out under the supervision of Engineer Tabarak Mohsin Ashour, aiming to introduce students to the scientific principles of recrystallization, proper solvent selection, and control of dissolution and crystallization conditions. This contributes to linking theoretical knowledge with practical learning and enhancing students’ laboratory skills, while ensuring compliance with approved laboratory safety procedures. This scientific activity aligns with the Sustainable Development Goals (SDGs), particularly: SDG 4: Quality Education, by supporting applied education and strengthening students’ scientific skills. SDG 9: Industry, Innovation, and Infrastructure, through preparing qualified students for research and development fields. SDG 12: Responsible Consumption and Production, by promoting the rational use of chemical materials and reducing laboratory waste.